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SECTION V PT PROCESS  CONTROL
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TM-1-1500-335-23 Nondestructive Inspection Methods Manual
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Frequency of Process Control Checks

T.O. 33B-1-1 1.5.1.3 Causes of Materials Degradation. 1.5.1.3.1 Materials Contamination. Materials contamination is a primary source of degrading the performance of a penetrant system.  There is a number of contaminating materials and their effect on performance depends upon the type of material.  Some of the common contaminants frequently encountered are: a. Water is probably the most common type of contaminant.  It can occur by careless or improper rinsing or carry over from other parts. b. Organic   materials   such   as   paint,   lubricants,   oils,   greases,   and   sealants   are   another   source   of contamination.  These materials, if not removed from parts during precleaning, can dissolve in the penetrant and react with or dilute it, so that it loses some or all of its ability to function. c. Organic  solvents  such  as  degreaser  f luid;  cleaning  solvent,  gasoline,  and  antifreeze  solution  are common types of contaminants.  These materials dissolve in the penetrant and reduce its effective- ness in proportion to the amount present.  A small change in performance is usually not noticeable (5% or less of the total volume).  The method of entry into penetrant is usually carry-over on the inside interior cavities of the part. d. Dirt,  soil  and  other  insoluble  solids  are  carried  into  the  penetrant,  emulsifier,  and  developer  as  a result  of  improper  precleaning  and  carry-over  from  other  parts.    Another  common  source  of  soil contamination occurs when the dwell stations are used to store parts.  Most dwell stations have drain pans, which return the eff luent back to the immersion tanks.  Any soil falling from unclean parts into the drain pan will be washed into the tank with the drain eff luent. e. Acid  and  alkaline  materials  are  serious  contaminants  of  penetrant  solutions.    They  react  with  the penetrant to destroy f luorescence brightness even when present in fairly small quantities.  They are usually residues from etching; plating or the cleaning processes. f. Penetrant is a normal contaminant of emulsifier in the postemulsifiable process.  It can be carried in on penetrant covered parts during the penetrant dwell step.  As the penetrant builds up in volume, it will gradually slow the emulsifying action, and if the level becomes high enough, the emulsification process will stop. 1.5.1.3.2 Evaporation Losses. Penetrant materials used in open tanks are continuously undergoing evaporation.  The rate of evaporation is increased with warmer temperatures and large tank surfaces.  Evaporation losses of penetrant result in an increase in viscosity, thus slowing penetration and emulsification.  Evaporation of water washable penetrant may  slow  or  speed  washability,  depending  on  the  penetrant  formula.    Evaporation  losses  in  developer solutions increase the concentration, which produces a heavier coating that may mask smaller indications. Since evaporation losses take place very gradually, performance change may become significant before it is noticed. 1.5.1.3.3 Heat Degradation. Penetrants,  especially  f luorescent  penetrants,  are  sensitive  to  elevated  temperatures.    Temperatures  over 140oF (60oC) can reduce the f luorescence; and temperatures over 250oF (121oC) may destroy it completely. High  temperatures  also  speed  evaporation  of  the  volatile  components  of  penetrants,  causing  undesired performance changes.  High temperatures in penetrants can occur from the following: a. Immersion of heated or hot parts. b. Inspection of surfaces exposed to the sun, such as f light line aircraft. c. Improper storage before being placed in use, such as storage in direct sunlight. 1.5.1.4 Process Degradation. Not only do materials degrade, but equipment and procedures (other elements of the process) can deteriorate also.    Black  light  bulbs  age  and  become  dirty,  reducing  their  output.    Drying  oven  thermostats  can  be improperly set or may malfunction, resulting in excessive temperatures which may cause critical procedures to  be  performed  incorrectly.    Materials,  equipment  and  procedures  SHALL  be  periodically  audited  during their service life to assure satisfactory process performance. Change 2 1-21

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