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Figure 1-5   AF Form 3130 Sample Format for Magnetic Particle Method Process Control
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TM-1-1500-335-23 Nondestructive Inspection Methods Manual
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Causes of Materials Degradation

T.O. 33B-1-1 1-20 SECTION V PT PROCESS  CONTROL 1.5 PENETRANT PROCESS CONTROL. This  section  provides  basic,  operating  and  advanced  level  information  on  the  procedures  necessary  to  assure  a  high quality performance from the penetrant inspection system.  The first part of the section discusses the reasons for process and materials control.  The second part describes procedures to verify materials quality.  The third part outlines review functions of the process. 1.5.1 Need For Process Quality. NOTE Materials   and   process   deficiencies   are   not   always   obvious.      It   is   not   easily determined that a penetrant has lost its ability to penetrate into a given flaw.  Thus, it  is  necessary  to  periodically  test  the  materials  and  to  inspect  the  equipment  and process to be sure they are functioning. Penetrant inspection, as well as all other nondestructive inspection processes, is not a perfect process.  The presence of indications  confirms  the  existence  of  discontinuities  in  the  part.    However,  the  absence  of  indications  does  not guarantee the absence of discontinuities.  Flaws can be present and not be indicated for a number of reasons.  The two main reasons for discrepancies in inspection results are: a.     Substandard   inspection   materials   due   to   either   receipt   of   bad   material   from   the   manufacturer   or degradation in storage or service. b.    Process deviations either in equipment, procedures, or conditions. 1.5.1.1 New Materials. Penetrant  materials  are  subjected  to  extensive  testing  during  their  formulation  to  assure  their  proper  composition. However,   materials   that   do   not   perform   satisfactorily   can   still   be   received.      Many   times,   the   discrepancies   in performance  have  not  been  detected  until  a  number  of  parts  have  been  processed.    Considerable  effort  must  then  be expended to locate and reinspect the suspect parts.  Unsatisfactory materials can result from a number of causes.  The penetrant supplier may inadvertently omit an ingredient or a process.  An ingredient with similar characteristics may be substituted   if   the   original   material   is   unavailable.      The   substitution   of   ingredients   may   occur   at   the   penetrant formulator’s  supplier.    Experience  has  shown  that  all  newly  received  penetrant  materials  must  be  tested  to  verify performance characteristics. 1.5.1.2 In-Use Materials. Some inspection processes use the penetrant materials one time with no attempt to recover the excess.  The materials are usually applied by spraying, and only enough material is applied to perform the test.  The materials are stored in closed   containers   until   they   are   used.      These   processes   minimize   the   possibility   of   material   contamination   or degradation  during  use.    More  often,  however,  the  materials  are  used  in  open  tanks  or  open  containers.    When  the immersion  method  is  used,  the  surplus  materials  are  allowed  to  drain  from  the  part  back  into  the  tank.    When  the materials  are  applied  by  brushing,  the  brush  is  alternately  stroking  the  part  surface  and  being  immersed  in  the container.    Both  methods  provide  numerous  opportunities  for  contamination  and  deterioration.    Materials  handled  in this manner must be checked periodically to be sure they are functioning acceptably.

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